![]() |
Macdonald Research Group |
| History & CV Teaching Publications Links Home Page | We
have a few labs that we are continuing to fill with equipment.
We have two glove boxes (a VAC dual-station dry box and an MBraun
single-station "wet" box), one of which is equipped with a
Leica stereo microscope for the mounting of crystals in capillaries for
X-ray diffraction studies. We use both Schlenk (inert gas) and
vacuum (Burford-Muller) glassware for the preparation and handling of our air-sensitive
compounds. We also have a solvent purification system in the lab
for the safe and efficient drying of solvents. In addition, we
have a variety of other standard laboratory equipment.
For theoretical calculations, we have a dual Xeon-processor Dell workstation and we have access to other workstations and clusters in the department.
We have access to many analytical tools, including: - 2 CCD detector equipped single-crystal X-ray diffractometers (one with VT-capability) - a Hi-Star area detector equipped powder X-ray diffractometer with VT-capability - multinuclear solution NMR spectrometers - a solid-state NMR spectrometer (through Prof. R. W. Schurko), - FT-IR, Raman, UV-vis and other spectrophotometers - a C,H,N elemental analyzer - thermal analysis equipment (DSC, TGA-MS) - separation/purification technology (LC-MS, GC, GPC) - other state-of-the-art facilities have recently been installed (AFM/STM, TOF-MS, multiple-quadrupole MS, and more) |